| CDCl3 | | 01 | 34.82 | | 02 | 36.90 | | 03 | 207.86 | | 04 | 39.62 | | 05 | 56.12 | | 06 | 198.19 | | 07 | 119.77 | | 08 | 158.64 | | 09 | 38.96 | | 10 | 37.43 | | 11 | 20.54 | | 12 | 38.99 | | 13 | 45.60 | | 14 | 71.91 | | 15 | 69.01 | | 16 | 29.48 | | 17 | 53.22 | | 18 | 15.81 | | 19 | 22.68 | | 20 | 38.30 | | 21 | 23.03 | | 22 | 133.54 | | 23 | 133.31 | | 24 | 43.12 | | 25 | 33.09 | | 26 | 19.74 | | 27 | 20.04 | | 28 | 17.74 |
|
| CDCl3 | | 01-Ha | 2.14 (ddd, 14.0, 6.8, 3.0) | | 01-He | 1.61 (td, 14.0, 4.9) | | 02-Ha | 2.53 (ddd, 16.0, 14.0, 6.8) | | 02-He | 2.37 (m) | | 04-Ha | 2.28 (dd, 14.9, 13.7) | | 04-He | 2.33 (m) | | 05-H | 2.43 (dd, 13.7, 5.3) | | 07-H | 6.06 (d, 2.6) | | 09-H | 2.93 (ddd, 7.8, 6.8, 2.6) | | 11-Ha | 1.81 (m) ? | | 11-He | ? | | 12-Ha | 1.68 (m) | | 12-He | 1.84 (m) | | 15-H | 3.18 (d, 2.0) | | 16-Ha | 2.03 (ddd, 15.2, 10.1, 2.0) | | 16-Hb | 2.09 (dd, 15.2, 3.7) | | 17-H | 1.72 (ddd, 15.2, 6.0, 3.7) | | 18-Me | 1.13 s) | | 19-Me | 1.08 (s) | | 20-H | 2.33 (m) | | 21-Me | 0.95 (d, 7.4) | | 22-H | 5.28 (dd, 15.6, 8.0) | | 23-H | 5.20 (dd, 15.6, 7.8) | | 24-H | 1.92 (d quintet, 7.8, 6.9) | | 25-H | 1.49 (octet, 6.9) | | 26-Me | 0.84 (d, 6.9) | | 27-Me | 0.86 (d, 6.9) | | 28-Me | 0.96 (d, 6.9) |
|